Almost all the constituent elements, including Fe as the major impurity, were leached out with high efficiencies in a single-step process using 2 M sulfuric acid at room temperature. A pH of 1.2 yielded complete precipitation …
Hybrid membrane process for the recovery of major components (zinc, iron and HCl) from spent pickling effluents ... We propose a hybrid membrane process consisting first of a liquid membrane step that generates a raffinate highly concentrated in iron chloride and a mixture of HCl and zinc chlorides in the stripping phase. Second, diffusion or ...
Selective leaching recovery for spent LiFePO 4 (LFP) has garnered significant attention owing to its advantages of low-cost, high-efficiency and eco-friendliness. Wherein, the separation effect of Li and Fe is particularly crucial. While previous studies have yielded effective Li-Fe separations experimentally, the migration behavior of Fe during the selective leaching process remains ...
This study confirmed the feasibility of using oxalic acid to recover iron from wet-processed phosphoric acid and prepare high purity ferrous oxalate, realizing high-value utilization of iron resources.
During the roasting-magnetic process of iron recovery, the red mud with other additives is commonly roasted in the form of separate pellets. ... The result suggests that the chemical reaction, rate-controlling step, plays a major role in the adsorption of the scandium ions using modified activated carbon. Mechanism of adsorption may be ...
When pyrite is used in the production of sulfuric acid, powdered pyrite cinder (PyC) is produced, which is usually small in size and contains some amount of iron [4], [23]. The major form of iron in PyC is Fe 2 O 3, and China's PyC iron grade is typically in the range of 30 % to 50 % (J. [13]; Z. [16]. PyC also contains harmful elements like Cu ...
Scandium is the 31st abundant element in the Earth's crust, with an average crustal abundance of 22 ppm (Hedrick, 2010b).Because it readily substitutes the major elements such as iron and aluminium, scandium rarely occurs in concentrated quantities, but distributes sparsely in trace amounts in rocks consisting of ferromagnesian minerals with an abundance of 5–100 ppm.
Direct acid leaching of bauxite residue for recovering REEs dissolves large amounts of major elements (iron, aluminum,..), which creates issues in further recovery process steps such as solvent extraction, ion exchange, etc. The generation of large volumes of effluents is also a major concern. Furthermore, direct acid leaching hardly reduces ...
In recent years, recovery of metals from spent lithium ion batteries (LIBs) has become increasingly important due to their high potential of environmental impacts and waste of valuable metallic ...
We conducted quantitative analysis of the recovery process during pure iron annealing using the modified Williamson-Hall and Warren-Averbach methods. We prepared …
The global shortage of zinc mines makes the extraction of zinc from zinc-containing wastes a hot research topic. Most kinds of steel mill dust (SMD) cannot be directly returned to the ironmaking and steelmaking …
For the reason of major iron recovery from copper slag, alkaline leaching with different molar concentrations of NaOH, Na 2 CO 3 and NaOH+Na 2 CO 3 salts was carried out that served the purpose of 85.74 % iron recovery from copper slag as shown in Fig. 4. The results indicated that, when the NaOH moles increased from 1 to 2 M, the residue's ...
Fig. 1 presents a diagram of example concepts of phosphorus recovery from sludge or leachates, together with the concentrations of major pollutants occurring there. The process of recovery after fermentation may be performed before (31% of recovery efficiency) or after the thickening process (85% of recovery efficiency).
(1) Well-established technology and reliable process (2) Fewer operation steps and simple process (3) High metallization rate of residue (1) High initial investment and operating costs (2) High operating temperature requirements: OxyCup: Zinc-rich dust; Molten iron; Slag (1) Many types of dust that can be recycled (2) High metal recovery rate
In addition, the combination of process such as the hydrometallurgy and electrolysis has been reported to improve the metal recovery process from e-waste [33,74, 75, 119]. ...
The underflow concentration of the two-step flocculation process was higher than that of any single flocculant. Compared to the widely-used flocculation process with a single polymer flocculant, this two-step process could not only significantly improve the total water recovery rate of the slurry, it could also produce a full re-growth of flocs.
Stage 5: Recovery. The incident response recovery phase revolves around testing the systems that were repaired, replaced, or reinforced during the eradication phase. Successful tests lead to resumed operations and service delivery. Like the first step in the standard incident recovery process, systems testing is a continuous cycle. As new ...
The recommended pH for iron precipitation was pH 3.5-4.0 with precipitate purity > 93.4% and iron recovery > 98.6%. AMD water after iron removal was used as source water for aluminum recovery.
30 °C; 130 rpm; two-step bioleaching process where the first step involves conversion of ferrous ions to their ferric counterpart in 48 h while the second step uses ferric ions for solubilization of Cu from PCBs. E-waste density 7.5 g/L: Benzal et al., 2020: 12. Cu (97.3 %), aluminium (55.8 %), Ni (79.3 %), Zn (66.8 %) from waste PCBs of ...
The recovery of lithium from spent lithium iron phosphate (LiFePO 4) batteries is of great significance to prevent resource depletion and environmental pollution.In this study, through active ingredient separation, selective leaching and stepwise chemical precipitation develop a new method for the selective recovery of lithium from spent LiFePO 4 batteries by using sodium …
Archambo and Kawatra, 2020, Archambo and Kawatra, 2020 studied iron recovery from high-iron RM by the nugget process in blast furnace, and the process flow diagram for the red mud iron nugget experiments was shown in Fig. 7. The optimal conditions for the roasting involved the treatment of high-iron RM (TFe grade of 50.97%) with 10% powdered ...
Separation and Recovery of Rare Earths and Iron from NdFeB Magnet Scraps ... two-step magnet separation process was implem ... (20193BCD40019), Academic and technical leaders of major disciplines in .
The recovery ratios of nickel and iron continuously increased from 82.53% to 92.44% and from 85.83% to 91.17%, respectively, as the magnetic intensity increased from 50 to 100 mT. As the magnetic intensity further increased, the recovery ratios of nickel and iron remained relatively constant.
Therefore, this paper initially focuses on long-stockpiled oxidized ores to validate the reliability of low-temperature fluidized reduction, comparing the effects of H 2 and CO as reducing gases on the recovery of iron, rare earths, and fluorite, and examining the changes in phase, magnetism, and pore structure of the oxidized ores during reduction. . Subsequently, the study uses …
± 3.57%. The novelty of the proposed environmentally friendly method is the recovery of iron in metallic electrolytic form and REEs in sulfate form, avoiding high temperature pyrometallurgical methods (roasting) or the use of additional chemical oxidizers. KEYWORDS: neodymium−iron−boron based magnets, rare earth elements recycling ...
The entire metal recovery process consists of three main steps: 1) mechanical pretreatment of waste, 2) metal leaching by an appropriate lixiviant, and 3) purification of …
Metallurgy - Refining, Alloying, Smelting: Refining is the final procedure for removing (and often recovering as by-products) the last small amounts of impurities left after the major extraction steps have been completed. It leaves the major metallic element in a practically pure state for commercial application. The procedure is accomplished in three ways: refining …
The hydrometallurgical recovery process is built on the separation of metals based on their chemical features in aqueous solutions (Liu et al., 2019a; Ye et al., 2017a). This method contains leaching procedure (acid/alkaline leaching, etc.), purification, and recovery process (extraction, precipitation, regeneration, etc.).
lateritic iron ore showed that the sample contained porous and friable oxides and hydroxides of iron. The ore sample had a feed grade of 54.43% total Fe, 9.27% SiO 2 and 8.02% Al 2O 3. Hematite and goethite are main iron-bearing minerals while kaolinite and gibbsite are the major gangue mineral constituents.
Synthesis of IONPs from ISA involved five major steps: burning of incense sticks to collect ISA, recovery of ferrous fractions from wet slurry by magnetic separation method, acidic treatment of ...